Dental Materials
Volume 25, Issue 6 , Pages 729-735 , June 2009

Demineralized dentin 3D porosity and pore size distribution using mercury porosimetry

  • Elsa Vennat

      Affiliations

    • Laboratoire Mécanique des Sols, Structures et Matériaux, Ecole Centrale Paris, Grande Voie des Vignes, 92295 Chatenay Malabry Cedex, France
    • Corresponding Author InformationCorresponding author. Tel.: +33 1 41 13 17 06.
    • ,
  • Christine Bogicevic

      Affiliations

    • Laboratoire Structures Propriétés et Modélisation des Solides, Ecole Centrale Paris, Grande Voie des Vignes, 92295 Chatenay Malabry Cedex, France
    • ,
  • Jean-Marie Fleureau

      Affiliations

    • Laboratoire Mécanique des Sols, Structures et Matériaux, Ecole Centrale Paris, Grande Voie des Vignes, 92295 Chatenay Malabry Cedex, France
    • ,
  • Michel Degrange

      Affiliations

    • Unité de Recherche Biomatériaux et Interfaces, Faculté de Chirurgie Dentaire, University Paris-Descartes, 1 rue Maurice Arnoux, 92120 Montrouge, France

Received 22 April 2008 ,Revised 15 December 2008 ,Accepted 17 December 2008.

References 

  1. Nakabayashi N, Kojima K, Masuhara E. The promotion of adhesion by infiltration of monomers into tooth substrates. J Biomed Mater Res. 1982;16:265–273
  2. Sano H, Shono T, Takatsu T, Hosoda H. Microporous dentin zone beneath resin-impregnated layer. Oper Dent. 1994;19:59–64
  3. Spencer P, Wang Y, Walker MP, Wieliczka DM, Swafford JR. Interfacial chemistry of the dentin/adhesive bond. J Dent Res. 2000;79:1458–1463
  4. Spencer P, Wang Y. Adhesive phase separation at the dentin interface under wet bonding conditions. J Biomed Mater Res. 2002;62:447–456
  5. Wang Y, Spencer P. Hybridization efficiency of the adhesive/dentin interface with wet bonding. J Dent Res. 2003;82:141–145
  6. Hashimoto M, Tay FR, Ohno H, Sano H, Kaga M, Yiu C, et al. SEM and TEM analysis of water degradation of human dentinal collagen. J Biomed Mater Res B Appl Biomater. 2003;66:287–298
  7. Yang B, Adelung R, Ludwig K, Böβmann K, Pashley DH, Kern M. Effect of structural change of collagen fibrils on the durability of dentin bonding. Biomaterials. 2005;26:5021–5031
  8. Breschi L, Mazzoni A, Ruggeri A, Cadenaro M, Di Lenarda R, De Stefano Dorigo E. Dental adhesion review: aging and stability of the bonded interface. Dent Mater. 2008;24:90–101
  9. Van Meerbeek B, Dhem A, Goret-Nicaise M, Braem M, Lambrechts P, VanHerle G. Comparative SEM and TEM examination of the ultrastructure of the resin-dentin interdiffusion zone. J Dent Res. 1993;72:495–501
  10. Tay FR, Moulding KM, Pashley DH. Distribution of nanofillers from a simplified-step adhesive in acid-conditioned dentin. J Adhes Dent. 1999;2:103–117
  11. Carvalho RM, Ciucchi B, Sano H, Yoshiyama M, Pashley DH. Resin diffusion through demineralized dentin matrix. Rev Odontol Univ São Paulo. 1999;13:417–424
  12. Habelitz S, Balooch M, Marshall SJ, Balooch G, Marshall GW. In situ atomic force microscopy of partially demineralized dentin collagen fibrils. J Struct Biol. 2002;138:227–236
  13. Figueiredo de Magalhães M, Neto Ferreira RA, Grossi PA, de Andrade RM. Measurement of thermophysical properties of human dentin: effect of open porosity. J Dent. 2008;36:588–594
  14. Nakabayashi N, Pashley DH. Hybridization of dental hard tissues. Tokyo: Quintessence Publishing Co. Ltd.; 1998;pp. 14–15
  15. Garberoglio R, Brännström M. Scanning electron microscopic investigation of human dentinal tubules. Arch Oral Biol. 1976;21:355–362
  16. Fosse G, Saele PK, Eide R. Numerical density and distributional pattern of dentin tubules. Acta Odontol Scand. 1992;50:201–210
  17. Pashley DH. Dentin: a dynamic substrate – a review. Scanning Microsc. 1989;3:161–174
  18. Driessens FCM, Verbeeck RMH. Biominerals. Boca Raton: CRC Press; 1990;pp. 163–178
  19. Moura MJ, Ferreira PJ, Figueiredo MM. Mercury intrusion porosimetry in pulp and paper technology. Powder Technol. 1995;160:61–66
  20. Kim SH, Chu CC. Pore structure analysis of swollen dextran-methacrylate hydrogels by SEM and mercury intrusion porosimetry. J Biomed Mater Res. 2000;53:258–266
  21. Milutinovic-Nikolic AD, Medic VB, Vukovic ZM. Porosity of different dental luting cements. Dent Mater. 2007;23:674–678
  22. Watson KE, Tenhuisen KS, Brown PW. The formation of hydroxyapatite-calcium polyacrylate composites. J Mater Sci Mater Med. 1999;10:205–213
  23. Hesaraki S, Sharifi D. Investigation of an effervescent additive as porogenic agent for bone cement macroporosity. Biomed Mater Eng. 2007;17:29–38
  24. Mueller HJ. Particle and pore size distributions of investments. J Oral Rehabil. 1986;13:383–393
  25. Carvalho RM, Yoshiyama M, Brewer PD, Pashley DH. Dimensional changes of demineralized human dentin during preparation for scanning electron microscopy. Arch Oral Biol. 1996;41:379–386
  26. Perdigao J, Lambrechts P, Van Meerbeek B, Vanherle G, Lopes ALB. Field emission SEM comparison of four postfixation drying techniques for human dentin. J Biomed Mater Res. 1995;29:1111–1120
  27. Webb PA, Orr C. Analytical methods in fine particle technology. Norcross: Micromeritics Instrument Corporation; 1997;
  28. Mikijelj B, Varela JA, Whittemore OJ. Equivalence of surface areas determined by nitrogen adsorption and by mercury porosimetry. Ceram Bull. 1991;70:829–831
  29. Mjör IA, Nordahl I. The density and branching of dentinal tubules in human teeth. Arch Oral Biol. 1996;41:401–412
  30. Kinney JH, Pople JA, Marshall GW, Marshall SJ. Collagen orientation and crystallite size in human dentin: a small angle X-ray scattering study. Calcif Tissue Int. 2001;69:31–37
  31. Nation JL. A new method using hexamethyldisilazane for preparation of soft insect tissues for scanning electron microscopy. Stain Technol. 1983;58:347–351

PII: S0109-5641(08)00301-1

doi: 10.1016/j.dental.2008.12.002

Dental Materials
Volume 25, Issue 6 , Pages 729-735 , June 2009

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