Dental Materials
Volume 23, Issue 5 , Pages 561-569 , May 2007

Qualitative analysis of adhesive interface nanoleakage using FE-SEM/EDS

  • Yang Yuan

      Affiliations

    • Department of Cariology and Operative Dentistry, Tokyo Medical and Dental University, Tokyo, Japan
    • Center of Excellence Program, FRMDRTB at TMDU, Tokyo, Japan
    • Corresponding Author InformationCorresponding author. Tel.: +81 3 5803 5483; fax: +81 3 5803 0195.
  • ,
  • Yasushi Shimada

      Affiliations

    • Department of Cariology and Operative Dentistry, Tokyo Medical and Dental University, Tokyo, Japan
  • ,
  • Shizuko Ichinose

      Affiliations

    • Instrumental Analysis Research Center, Tokyo Medical and Dental University, Tokyo, Japan
  • ,
  • Junji Tagami

      Affiliations

    • Department of Cariology and Operative Dentistry, Tokyo Medical and Dental University, Tokyo, Japan
    • Center of Excellence Program, FRMDRTB at TMDU, Tokyo, Japan

Received 14 June 2005 ,Revised 7 February 2006 ,Accepted 9 March 2006.

References 

  1. Van Meerbeek B, Perdigão J, Lambrechts P, Vanherle G. The clinical performance of adhesives. J Dent. 1998;26(1):1–20
  2. Pashley DH, Carvalho RM. Dentine permeability and dentine adhesion. J Dent. 1997;25:355–372
  3. Sano H, Yoshiyama M, Ebisu S, Burrow MF, Takatsu T, Ciucchi B, et al. Comparative SEM and TEM observations of nanoleakage within the hybrid layer. Oper Dent. 1995;20:160–167
  4. Sano H, Takatsu T, Ciucchi B, Horner JA, Matthews WR, Pashley DH. Nanoleakage: leakage within the hybrid layer. Oper Dent. 1995;20:18–25
  5. Li H, Burrow MF, Tyas MJ. Nanoleakage patterns of dentin bonding system. Dent Mater. 2000;16:48–56
  6. Pioch T, Staehle HJ, Duschner H, Garcia-Godoy F. Nanoleakage at the composite–dentin interface: a review. Am J Dent. 2001;14:252–258
  7. Tay FR, Pashley DH, Yoshiyama M. Two modes of nanoleakage expression in single-step adhesives. J Dent Res. 2002;81(7):472–476
  8. Van Meerbeek B, De Munck J, Yoshida Y, Inomue S, Vargas M, Vijay P, et al. Buonocore memorial lecture—adhesion to enamel and dentin: current status and future chllenges. Oper Dent. 2003;28(3):215–235
  9. Sano H, Yoshikawa T, Pereira PNR, Kanemura N, Morigami M, Tagami J, et al. Long-term durability of dentin bonds made with a self-etching primer, in vivo. J Dent Res. 1999;78(4):906–911
  10. Pereira PN, Okuda M, Nakajima M, Sano H, Tagami J, Pashley DH. Relationship between bond strengths and microleakage: evaluation of a new assessment method. Am J Dent. 2001;14:100–104
  11. Kubo S, Li H, Burrow MF, Tyas MJ. Nanoleakage of dentin adhesive systems bonded to carisolv-treated dentin. Oper Dent. 2002;27:387–395
  12. Tay FR, Moulding KM, Pasheley DH. Distribution of nanofillers from a simplified-step adhesive in acid-conditioned dentin. J Adhes Dent. 1999;2:103–117
  13. Eick JD, Miller RG, Robinson SJ, Bowles CQ, Gutshall PL, Chappelow CC. Quantitative analysis of the dentin adhesive interface by auger spectroscopy. J Dent Res. 1996;75(4):1027–1033
  14. Hashimoto M, De Munck J, Ito S, Sano H, Kaga M, Oguchi H, et al. In vitro effect of nanoleakage expression on resin–dentin bond strengths analyzed by microtensile bond test, SEM/EDS TEM. Biomaterials. 2004;25:5565–5574
  15. Tay FR, Kwong SM, Itthagarun A, King NM, Yip HK, Moulding KM, et al. Bonding of a self-etching primer to non-carious cervical sclerotic dentin: interfacial ultrastructure and microtensile bond strength evaluation. J Adhes Dent. 2002;2:9–28
  16. Paul SJ, Welter DA, Ghazi M, Pashley DH. Nanoleakage at the dentin adhesive interface vs μ-tensile bond strength. Oper Dent. 1999;24:181–188
  17. Tay FR, King NM, Chan KM, Pashley DH. How can nanoleakage occur in self-etching systems that demineralize and infiltrate simultaneously?. J Adhes Dent. 2002;4:255–269
  18. Hashimoto M, Ito D, Tay FR, Sviaero NR, Sano H, Kaga M, et al. Fluid movement across the resin–dentin interface during and after bonding. J Dent Res. 2004;83(11):843–848
  19. Fernando de Goes M, Montes MA. Evaluation of silver methenamine method for nanoleakage. J Dent. 2004;32:391–398
  20. Carvalho RM, Chersoni S, Frankenberger R, Pashley DH, Prati C, Tay FR. A challenge to the conventional wisdom that simultaneous etching and resin infiltration always occurs in self-etch adhesives. Biomaterials. 2005;26:1035–1042
  21. Yoshida Y, Nagakane K, Fukuda R, Nakayama Y, Okazaki M, Shintani H, et al. Comparative study on adhesive performance of functional monomers. J Dent Res. 2004;83(6):454–458
  22. Tay FR, Pashley DH. Have dentin adhesives become too hydrophilic?. J Can Dent Assoc. 2003;69(11):726–731
  23. Tay FR, Pashley DH, Suh BI, Carvalho RM, Itthagarun A. Single-step adhesives are permeable membranes. J Dent. 2002;30:371–382
  24. Carvalho RM, Mendonca JS, Santiago SL, Silveira RR, Garcia FC, Tay FR, et al. Effects of HEMA/solvent combinations on bond strength to dentin. J Dent Res. 2003;82(8):597–601
  25. Spencer P, Wang Y. Adhesive phase separation at the dentin interface under wet bonding conditions. J Biomed Mater Res. 2002;62:447–456
  26. Tay FR, Gwinnett AJ, Wei SH. Micromorphological spectrum from overdrying to overwetting acid-conditioned dentin in water-free, acetone-based, single-primer/adhesives. Dent Mater. 1996;12:236–244
  27. Van Landuyt KL, De Munck J, Sanuwaert J, Coutinho E, Poitevin A, Yoshida Y, et al. Monomer-solvent phase separation in one-step self-etch adhesives. J Dent Res. 2005;84(2):183–188
  28. Tay FR, Sano H, Tagami J, Hashimoto M, Moulding KM, Yiu C, et al. Ultrastructural study of a glass ionomer-based, all-in-one adhesive. J Dent. 2001;29:489–498
  29. Tay FR, Pashley DH, Yiu C, Cheong C, Hashimoto M, Itou K, et al. Nanoleakge types and potential implications: evidence from unfilled and filled adhesive with the same resin composition. Am J Dent. 2004;17:182–190
  30. Tagami J, Tao L, Pashley DH. Correlation among dentin depth, permeability, and bond strength of adhesive resins. Dent Mater. 1990;6:45–50
  31. Davidson CL, Abadalla AI. Effect of occlusal load cycling on the marginal integrity of adhesive class V restorations. Am J Dent. 1994;7:111–114
  32. Shimada Y, Tagami J. Effects of regional enamel and prism orientation on resin bonding. Oper Dent. 2003;28:20–27
  33. Wang H, Shimada Y, Tagami J. Shear bond stability of current adhesive systems to enamel. Oper Dent. 2004;29(2):168–175
  34. Tagami J, Sugizaki J, Hosoda H. Effect of various pretreatments for dentin bonding on dentin permeability. Jpn J Dent Mater. 1990;9:240–246
  35. Okuda M, Pereira PN, Nakajima M, Tagami J. Relationship between nano-leakage and long-term durability of dentin bonds. Oper Dent. 2001;26:482–490
  36. Okuda M, Pereira PN, Nakajima M, Tagami J, Pashley DH. Long-term durability of resin dentin interface: nano-leakage vs. microtensile bond strength. Oper Dent. 2002;27:289–296

PII: S0109-5641(06)00103-5

doi: 10.1016/j.dental.2006.03.015

Dental Materials
Volume 23, Issue 5 , Pages 561-569 , May 2007